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7. Use the spectroscopic data on the next page to determine the structure in the center...
A compound of unknown structure gave the following spectroscopic data: Mass spectrum: M+ = 88.1 IR:...
A compound of unknown structure gave the following
spectroscopic data:
Mass spectrum: M+ = 88.1
IR: 3600cm-1
1H NMR: 1.4 (2H, quartet, J=7Hz); 1.2 (6H, singlet); 1.0 (1H,
singlet); 0.9 (3H, triplet, J=7Hz)
13C NMR: 74, 35, 27, 25
a. assuming that the compound contains C and H but may or may not
contain O, give three possible molecular formulas.
b. how many protons (H) does the compound contain?
c. what functional group(s) does the compound contain?
d. how many...
Task Determine the structure of the molecules and comment on the spectroscopic data. Bruttoformel: C5H10BrN 1H...
Task Determine the structure of the molecules and comment on the spectroscopic data. Bruttoformel: C5H10BrN 1H NMR, ppm: 4,24 (kvintet, J = 7 Hz, 1H); 2,88 (kvartet, J = 7 Hz, 4H); 2,40 (singlet, 1H); 2,03 (triplet, J = 7 Hz, 4 H). 13C NMR, ppm: 50,2; 45,2#; 37,3#. IR, cm-1: 3370 (m), 2890 (m), 1105 (m).
9. Use the NMR data and chemical formula to determine the structure of the molecule. a) Formula: C5H100 TH NMR 13C...
9. Use the NMR data and chemical formula to determine the structure of the molecule. a) Formula: C5H100 TH NMR 13C NMR triplet quartet 200 180 160 140 30 60 40 20 0 120 100 Am b) Formula: C3H100 TH NMR 13C NMR singlet singlet doublet doublet 2 2 3 3 8 2 00 180 160 140 120 100 30 60
2. Use the 'H NMR and IR data to determine the structure of the following compounds...
2. Use the 'H NMR and IR data to determine the structure of the following compounds and name them. Compound A Molecular formula: CroH IR absorptions at N/A H NMR data: 1.3 (singlet, 9H), 7.0 to 7.5 (multiplet, 5H) ppm Compound B Molecular formula: CHO IR absorptions at 1H NMR data: 1735-1745, 1050 cm 0.93 (doublet, 6H), 1.52 (multiplet, 2H), 1.69 (multiplet, 1H), 2.04 (singlet, 3H), and 4.10 (triplet,2H) ppm Compound C Molecular ion: IR absorptions at 1710 cm 1H...
2. Draw the structure of the major organic product that is formed from the following reaction....
2. Draw the structure of the major organic product that is formed from the following reaction. Draw this structure in the box at the bottom of the next page. Then use letters to label all the sets of chemically equivalent carbons in this structure. The broadband proton-decoupled 13C NMR spectrum of the product is shown below. DEPT 90 and DEPT 135 data are included in the table on the following page. Use this spectroscopic data to make clear assignments of...
PART 3 For each set of data on pages 5-9, calculate and record the degree of...
PART 3 For each set of data on pages 5-9, calculate and record the degree of unsaturation. Then use your problem solving skills to determine the chemical structure that is consistent with ALL of the data on each page. You are not required to label the spectra (but feel free to do so). This entire assignment is to be completed independently Suggestion for a general method to determine a chemical structure based on the provided molecular formula, IR, H-NMR and...
A compound of unknown structure gave the following
spectroscopic data:
Mass spectrum: M+ = 88.1
IR: 3600cm-1
1H NMR: 1.4 (2H, quartet, J=7Hz); 1.2 (6H, singlet); 1.0 (1H,
singlet); 0.9 (3H, triplet, J=7Hz)
13C NMR: 74, 35, 27, 25
a. assuming that the compound contains C and H but may or may not
contain O, give three possible molecular formulas.
b. how many protons (H) does the compound contain?
c. what functional group(s) does the compound contain?
d. how many...
9. Use the NMR data and chemical formula to determine the structure of the molecule. a) Formula: C5H100 TH NMR 13C NMR triplet quartet 200 180 160 140 30 60 40 20 0 120 100 Am b) Formula: C3H100 TH NMR 13C NMR singlet singlet doublet doublet 2 2 3 3 8 2 00 180 160 140 120 100 30 60
2. Use the 'H NMR and IR data to determine the structure of the following compounds and name them. Compound A Molecular formula: CroH IR absorptions at N/A H NMR data: 1.3 (singlet, 9H), 7.0 to 7.5 (multiplet, 5H) ppm Compound B Molecular formula: CHO IR absorptions at 1H NMR data: 1735-1745, 1050 cm 0.93 (doublet, 6H), 1.52 (multiplet, 2H), 1.69 (multiplet, 1H), 2.04 (singlet, 3H), and 4.10 (triplet,2H) ppm Compound C Molecular ion: IR absorptions at 1710 cm 1H...
2. Draw the structure of the major organic product that is formed from the following reaction. Draw this structure in the box at the bottom of the next page. Then use letters to label all the sets of chemically equivalent carbons in this structure. The broadband proton-decoupled 13C NMR spectrum of the product is shown below. DEPT 90 and DEPT 135 data are included in the table on the following page. Use this spectroscopic data to make clear assignments of...
PART 3 For each set of data on pages 5-9, calculate and record the degree of unsaturation. Then use your problem solving skills to determine the chemical structure that is consistent with ALL of the data on each page. You are not required to label the spectra (but feel free to do so). This entire assignment is to be completed independently Suggestion for a general method to determine a chemical structure based on the provided molecular formula, IR, H-NMR and...
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