I need help with a 2-part organic chemistry lab. The main topic is esterification of fatty acids.
In the reaction, I mix acetic acid, ethanol, and diethyl ether (solvent) together and then add the reagent (H2SO4) to the flask. The final product of this reaction is ethyl acetate. Ethyl acetate is then extracted in a separatory funnel using NaOH.
For this reaction, I need help with 2 things. I need help with the overall reaction mechanism, and in identifying the role of each component that is added. Why is ethyl acetate extracted with NaOH? What does the NaOH do?
I need help with a 2-part organic chemistry lab. The main topic is esterification of fatty...
I need help with an organic chemistry lab. The main topic is Ester Hydrolysis. I start with 1,7-Dimethylhaptanedioate and water (solvent), and add the catalyst H2SO4. The reaction mixture is extracted with water. The final product is heptanedioic acid. I need to know the steps of the reaction mechanism, as well as the role of each component in the reaction. I also need to know why the reaction mixture is extracted with water, and what the water does. Why water...
Esterification of benzyl acetate - Limiting Reagent and Reaction Help In my lab, we synthesized benzyl acetate from sodium acetate and benzyl bromide. We used 1.5 g of sodium acetate and 0.9 equivalents of benzyl bromide (2.81 g which was in liquid form so 1.95 mL) with 10 mL of DMF solvent (+ water to quench). I need help with what the reaction is and then what the limiting reagent would be. Thanks!
Organic Chemistry Lab question In the experiment we did acid-base extractions to find impurities. The impurity was either benzoic acid (acid) or 4-chloroaniline (base) So in this experiment we did Acid-Base extraction with an unknown compound. So we had an unknown of 0.150 grams and mixed it with 20 mL of diethyl ether. We placed this in a separatory funnel and added 2mL of 1.0 NaOH solution to the separatory funnel and placed the stopper over the top of the...
Need help on providing reactions that describe the acid-base
extraction and neutralization processes used in this experiment.
Provide a statement of solubility of each starting material and
product.
The experiment to be performed this week involves liquid-liquid extraction using a separatory funnel. Read chapter 15 in Zubrick to familiarize yourself with the use of the glassware for extraction and washing. Acid/Base Extraction Liquid-liquid extraction is a technique that can be used to physically separate two substances that have varying solubility...
I need to write out a procedure for extraction and recrystallization of a 1:1 (by mass) mixture of 1,4-dichlorobenzene/ethyl 4-aminobenzoate. So far, I have that I am starting with extraction using 1 g. of the mixture and dissolving it in about 15mL of diethyl ether. Then I am putting it in a separatory flask and adding 15mL of 1M HCl to get layers. To the organic layer, I will add sodium sulfate and put in rotovap to get a solid....
You are working in a chemistry lab that makes food additives and you are tasked with preparing 9.50 grams of butyl acetate for candy production. You know that esters can be prepared using Fischer esterification, and so choose to use that method to synthesize your target compound. Your reaction mixture is set up as follows: Add the alcohol (1.0 equivalent), carboxylic acid (1.3 equivalents) and H2SO4 (0.35 equivalents) to the Erlenmeyer flask. (Note that H2SO4 is an 18 M solution)....
Hello, I need help understanding a lab we are doing in class tomorrow. I need to know which is the "ORGANIC LAYER" ... we are using a separatory funnel, and I would like to know whether the organic layer will be on top or on the bottom. This is in order for me to correctly carry out the experiment. The lab is similar to this one I found online, and its very vague for me as to what is the...
Hi, I need help with somthing in my organic chemistry lab. We are supposed to prepare a .15M copper acetate acetic acid solution (.12 equiv) and ammonium nitrate (1.5 equiv). we have to make this based off our benzoin, which is 1.0 equiv and .942 mmol. Would you please be able to show all the work!
Organic chemistry post-lab question: "Why is important
to add the alkyl halide dropwise in your reaction? (Hint: your
reaction is not heated, but you still need a water-cooled
condenser!)" Please answer in detail!
Here is a copy of the experiment, thank you!
The Grignard reaction is an important synthetic process by which a carbon-carbon bond is formed. Magnesium metal is first reacted with an organic halide. The resultant organo-magnesium halide (Grignard reagent) is then combined with a carbonyl compound, ultimately...
Please can someone help me to interpret this. This was
from Orgo II Williamson ether Lab. These are the results and I need
help interpreting what this is showing. More especially for the
discussion and conclusion section. Thank You!
(if needed here are the procedures)
Add a magnetic stir bar to a 25ml round or pear-shaped
flask.
Add guaiacol (0.55ml,5mmoles) to the flask along with 3ml of
95% ethanol. Make sure the guaiacol dissolves in the ethanol before
proceeding.
Add...