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How do you determine the estimated loss in washing? Thank you! weight of watch glass and...

How do you determine the estimated loss in washing? Thank you!

weight of watch glass and salicylic acid 44.56 g
weight of empty watch glass 42.51 g
weight of salicylic acid 2.05 g
volume of acetic anhydride 3.0 ml
volume of concentrated sulfuric acid 5 drops
time of heating 21 min
total amount of water added to product

35 ml

weight of filter paper plus product 24.74 g
weight of dry filter paper 22.31 g
weight of product 2.43 g
theoretical yield (based on limiting reagent 2.674 g
percent yield 90.88%
Estimated loss in washing (at 3.3 mg/ mL)

?

Melting point of product 156.3 C
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