1) H2SO4 is a very strong and volatile acid. Skin contact causes damage, in addition to inhalation. You have to wear protection and do it in a hood.
2) It is an astringent substance, which in its excess can be harmful, protection should be used to handle and wash it.
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SYNT 451: Synthesizing Alum name Pre-Laboratory Ass 1. (1) What precautions should you take when you...
Pre-Laboratory Assignment • What particular precautions should you take 3. Methyl alcohol, CH,OH, reacts with benzoic acic when doing the following: CHECO,H, to form an ester. (1) using concentrated sulfuric acid (1) Using structural formulas, write the equatic for this reaction. (2) using glacial acetic acid (3) using a warm-water bath (2) What is the name of this ester? (4) Smelling ester odors 2. What is the purpose of the concentrated sulfuric acid used in this experiment?
1. A patient under isolation precautions is being transported to the x-ray department. He has no mask on and sneezes in the elevator. This scenario is an example of what type of hazard? A. Chemical hazard B. Sharps hazard C. Chain-of-infection hazard D. Physical hazard 2. What is the best procedure for removing gloves when leaving the laboratory? A. Take gloves off last and leave. B. Take gloves off and wash hands. C. Leave gloves on and remove them outside...
Name Pre-Laboratory Questions #9 - Anions Due at the beginning of lab! (2 pts) 1. You mix a solution of Na SO, with BaCl2 and a precipitate forms. What is the next step? 2. What observation are you looking for when nitric acid is added to a precipitate? 3. Reference the solubility rules from experiment #5. Will Na2SO4 form a precipitate when combined with BaCl2? 4. Reference the solubility rules from experiment #5. Will NaCl form a precipitate when combined...
name 1. Briefly doscribe Pre-Laboratory Assignment 3. Write the chemical equation(s) for each part the experimet, as outlined in Equation 1 the (a) why you must carry out the oxidation of Cu oxidation of Cu b) Part ! (b) why you should be particularly careful when you work with 3M H2SO4 solution. 2. Briefly explain the meaning of each of the tol lowing terms as it relates to this experiment. (a) decant (b) filtrate (c) supernatant liquid
Pre-Laboratory Assignment 1. What safety precautions must be observed when using (a) pyridinium tribromide? (b) acetic acid? 2. Calculate the theoretical yield for the bromination of both stilbenes and cinamic acid, assuming the presence of excess pyridinium tribromide. Note the theoretical yields here and in your laboratory notebook 3. Draw the mechanism, including the intermediate bromonium ion, generated in the bromination of trans-2-butene. 4. (a) Look up and draw structures for cinnamic acid, cis-stilbene, and trans-stilbene. (b) Predict the relative...
1. A patient under isolation precautions is being transported to the x-ray department. He has no mask on and sneezes in the elevator. This scenario is an example of what type of hazard? A. Chemical hazard B. Sharps hazard C. Chain-of-infection hazard D. Physical hazard 2. What is the best procedure for removing gloves when leaving the laboratory? A. Take gloves off last and leave. B. Take gloves off and wash hands. C. Leave gloves on and remove them outside...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
Preparation of Aspirin Name Class & Section PRE-LABORATORY ASSIGNMENT 1. What hazards should you be aware of when working with the following chemicals? a. Acetic anhydride b. Concentrated sulfuric acid 2. Explain the following terms as they relate to this experiment. a. Catalyst b. Limiting reactant 3. Following the procedure described in this experiment, a student reacted 2.775 g of salicylic acid with 4.0 ml of acetic anhydride and recovered 2.986 g of aspirin. a. Calculate the number of moles...
Name Section/CRN EXPERIMENT 12: PLASTICS AND POLYMERS PRE-LABORATORY-QUESTIONS : The following preparatory questions should be answered before coming to lab. They : are intended to introduce you to several ideas that are important to aspects of the experiment. You must turn in your work to your instructor before you will be allowed to begin the experiment. 1. What is the difference between polymer and plastic? 2. a) Give one use of the polymer Nylon. b) What is the polymer found...
Synthesis of 1-Bromobutane: An SN2 Reaction Pre-Laboratory
Exercises
PRE-LABORATORY EXERCISES NAME: Cynthesis of 1-Bromobutane: An SN 2 Reaction Butylbromide was prepared by refluxing in a 100-ml round bottomed flask a solution containing 13:35 Br 15 ml of water, 10 mL of n-butyl alcohol. 15 ml of concentrated H.SO. and a few boiling stories, 1. 2. R." d 1.275 laborales Nel CH3CH2CH2CH2OH + NaBr H2SO4 Superletalyst CHCH2CH2CHBr + NaHSO + HO (eq. 16) 1-butanol bp 118 C 1-bromobutane d 0.810 bp...