C8H12O4: DU= 2(8)+2-12/2= 3
Compound is that CH3CH2OOCCH=CHCOOCH2CH3
Diethylfumarate or diethylmaleate.
CNMR: CH3- 14.6 , CH2- 62.3& =CH-130.3, C=O- 166.5
IR: 3100 for =CH stretch and at 2986 cm-1 for CH stretch and at 1725 for C=O stretch and at 1620 for C=C strech and at 1160 for C-O stretches.
HNMR: 6.80 , doublet, 2H, 4.30 , quartet 4H and 1.35 , triplet, 6H(2x3H)
Find the molecular structure Unknown 7, CSH12O4 OT 200 180 160 140 120 100 80 60...
Check 200 180 160 120 80 60 40 20 0 140 a 100 ppm s, 3H t, 3 H d. 2 a. 2 H d. 2H s, 1 H 1 10 9 8 7 6 4 3 2 1 5 ppm 1) Which compound gives the following spectra? For the 'H-NMR assign all signals. Interpret mol peak and base peak in the mass spectrum if a mole peak exists. Assign at least two 13C signals, How does the IR spectrum...
Given the spectra determine the molecular formula and structure
m/z = 171
Unknown 1H 13C-NMR 160 210 190 180 110 80 50 20 200 170 150 140 130 100 40 10 240 230 220 120 f1 (opm) 60 30 -125.65 Unknown 1H 'H-NMR expansion 7.55 7.50 745 7.30 7.90 7.85 7,75 7,70 765 7.60 7.35 7.25 7,15 7BC 740 7.20 7,10 f1 (opm) PerkinElmer Spectrum Version 10.03.09 Friday, 8 March 2019 2:51 PM Analyst Analyst3 Friday, 8 March 2019 2:51...
180 140 100 200 160 120 80 60 40 20 11 10 9 6 pm 7 3 2 ppm 100- 80- 60- 40- 20- 75 100 125 150 25 50 m/z Relative Intensity o Write all of your notes on the spectra Type a justification of each structure in the same order they appear in your stapled packet o Insert page breaks so each structure is on a separate page o Include page numbers o Type your name in the...