Estimate the amount of product that was lost in the filtrate, assuming that the volume of...
Estimate the amount of product that was lost in the filtrate, assuming that the volume of the reaction mixture was 5.0 mL when you collect the product by vacuum filtration. Compare with with the amount of prodcut you would have lost if you had not boiled off most of the water. The solubility of the product is 6.8 g/100 mL at 20C.
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Estimate the amount of product that was lost in the filtrate,
assuming that the volume of...
can someone explain to me what exactly is going on in this lab? like what does...
can
someone explain to me what exactly is going on in this lab? like
what does benzyltriphenylphosphonium chloride, trans-cinnamaldehyde
and water do ? why was NaOH used? we produced
1,4-diphenyl-1,3-butadiene
Procedure: Place 2.10 mmol benzyltriphenylphosphonium chloride (Calculate BEFORE you come to the lab and know how many grams you need!) and 2.00 mmol trans-cinnamaldehyde (Calculate BEFORE you come to the lab and know how many ml you need. Use the molecular weight and the density for your calculation.) in a...
For the nitration of methyl benzoate: a. Which product did you get? What evidence do you...
For the nitration of methyl benzoate:
a. Which product did you get? What evidence do you have for
this?
b. Was your product pure? What evidence do you have for this?
Explain your evidence.
c. Draw the mechanism for the product you got.
For the bromination of acetanilide:
a. Which product did you get? What evidence do you have for
this?
b. Was your product pure? What evidence do you have for this?
Explain your evidence.
c. Draw the mechanism...
Naphthol was used in place of naphthalene. The product that resulted was 2-nitro-1-naphtol which was determined...
Naphthol was used in place of naphthalene. The product
that resulted was 2-nitro-1-naphtol which was determined by
comparing the melting points. I'm unsure of the mechanism for the
reaction with the flow of electrons
Measure 2.0 ml, of the mixed acid (1:l sulfuric acid and nite a small test tube or a conical vial. In small pottions, add divided naphthalene to the mixed acid, stirring or shaking each addition and cooling [OP-8] as nece around 45-S0°C. Then stit or shake...
Place 3.0 g of salicylic acid in a 125-ml Erlenmeyer flask. Carefully add, stirring constantly, 6...
Place 3.0 g of salicylic acid in a 125-ml Erlenmeyer flask. Carefully add, stirring constantly, 6 mL of acetic anhydride, followed by 10 drops of concentrated sulfuric acid. Swirl the contents of the flask so that the reactants are thoroughly mixed. Stopper the flask with a one- hole cork fitted with an inverted Pasteur pipet to prevent condensation of water in the reaction flask during heating on the steam bath. Heat the flask in a boiling-water or steam bath for...
Complete the table of reactants and products for the following two reactions. Compound Molar Mass (g/mol)...
Complete the table of reactants and products for the following two reactions. Compound Molar Mass (g/mol) Mass Volume Density (g/mL) # Mols Equivalents of Reactants (divide actual moles by stoichiometric moles) Other (indicate which is limiting reactant) Nitration of Methyl Benzoate In a 50 mL Erlenmeyer flask, cool 6 mL of conc. H2SO4 in ice and add 3.0 g of methyl benzoate. Make sure the temperature stays at 0 oC . Using a pipet, slowly add a cooled mixture of...
Running the Reaction Add 0.100 g benzil and 0.30 mL 95% ethanol to a 3-mL conical vial. Place a s...
Determine the theoretical yield and limiting reagent
Running the Reaction Add 0.100 g benzil and 0.30 mL 95% ethanol to a 3-mL conical vial. Place a spin vane in the vial and attach an air condenser. Heat the mixture with an aluminum block (90-100°C) while stirring until the benzil has dissolved (see inset in Tech- nique 6, Figure 6.1A). Using a 9-inch Pasteur pipette, add dropwise 0.25 mL of an aqueous potassium hydroxide solution' downward through the condenser into the...
RTY Uno Collect the recrystallized product by vacuum filtration with the clamped Hirsch funnel and wash...
RTY Uno Collect the recrystallized product by vacuum filtration with the clamped Hirsch funnel and wash the crystals with 1 mL of cold, 50% aqueous ethanol. Then allow the crystals to air dry until the next laboratory period. Percent Yield and Characterization Weigh the dry product and calculate a percent yield. Then determine its melting point range and compare the result with the literature value. Submit the product in a labeled plastic bag with the report Questions 1. Use the...
Can you explain how to find what is the theoretical yield, and the desired percent yield...
Can you explain how to find what is the theoretical yield, and
the desired percent yield of ethyl 4-nitrobenzoate?
1. Synthesis of ethyl 4-nitrobenzoate a) In a 50-ml round-bottom flask, weigh out 4-nitrobenzoic acid (0.85 g, 0.005 mol). Add to this 8 ml of absolute ethanol. Add boiling stones, and then bring this solution to the Lab Technologist. WATER OUT b) The Lab Technologist will deliver 1.2 ml of concentrated sulfuric acid to the mixture from the automatic pipette. [CAUTION,...
question 2 and 6 thabk you Exercises 1. (a) Calculate the volume of 6 M NaOH...
question 2 and 6 thabk you
Exercises 1. (a) Calculate the volume of 6 M NaOH required to react completely with the amount of methyl salicylate you used. How much of the 6 M NaOH that you used was in excess of the theoretical amount? (b) What volume of 3 M H SO is needed to neutralize all of the disodium salicylate and the excess NaOH present after the initial reaction? How much sulfuric acid was in excess? 2. Refer...
what is the theoretical yield of anisalacetophenone and dibenzalacetone formed? thank you. The Aldol Condensation Precautions:...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
can
someone explain to me what exactly is going on in this lab? like
what does benzyltriphenylphosphonium chloride, trans-cinnamaldehyde
and water do ? why was NaOH used? we produced
1,4-diphenyl-1,3-butadiene
Procedure: Place 2.10 mmol benzyltriphenylphosphonium chloride (Calculate BEFORE you come to the lab and know how many grams you need!) and 2.00 mmol trans-cinnamaldehyde (Calculate BEFORE you come to the lab and know how many ml you need. Use the molecular weight and the density for your calculation.) in a...
For the nitration of methyl benzoate:
a. Which product did you get? What evidence do you have for
this?
b. Was your product pure? What evidence do you have for this?
Explain your evidence.
c. Draw the mechanism for the product you got.
For the bromination of acetanilide:
a. Which product did you get? What evidence do you have for
this?
b. Was your product pure? What evidence do you have for this?
Explain your evidence.
c. Draw the mechanism...
Naphthol was used in place of naphthalene. The product
that resulted was 2-nitro-1-naphtol which was determined by
comparing the melting points. I'm unsure of the mechanism for the
reaction with the flow of electrons
Measure 2.0 ml, of the mixed acid (1:l sulfuric acid and nite a small test tube or a conical vial. In small pottions, add divided naphthalene to the mixed acid, stirring or shaking each addition and cooling [OP-8] as nece around 45-S0°C. Then stit or shake...
Place 3.0 g of salicylic acid in a 125-ml Erlenmeyer flask. Carefully add, stirring constantly, 6 mL of acetic anhydride, followed by 10 drops of concentrated sulfuric acid. Swirl the contents of the flask so that the reactants are thoroughly mixed. Stopper the flask with a one- hole cork fitted with an inverted Pasteur pipet to prevent condensation of water in the reaction flask during heating on the steam bath. Heat the flask in a boiling-water or steam bath for...
Determine the theoretical yield and limiting reagent
Running the Reaction Add 0.100 g benzil and 0.30 mL 95% ethanol to a 3-mL conical vial. Place a spin vane in the vial and attach an air condenser. Heat the mixture with an aluminum block (90-100°C) while stirring until the benzil has dissolved (see inset in Tech- nique 6, Figure 6.1A). Using a 9-inch Pasteur pipette, add dropwise 0.25 mL of an aqueous potassium hydroxide solution' downward through the condenser into the...
RTY Uno Collect the recrystallized product by vacuum filtration with the clamped Hirsch funnel and wash the crystals with 1 mL of cold, 50% aqueous ethanol. Then allow the crystals to air dry until the next laboratory period. Percent Yield and Characterization Weigh the dry product and calculate a percent yield. Then determine its melting point range and compare the result with the literature value. Submit the product in a labeled plastic bag with the report Questions 1. Use the...
Can you explain how to find what is the theoretical yield, and
the desired percent yield of ethyl 4-nitrobenzoate?
1. Synthesis of ethyl 4-nitrobenzoate a) In a 50-ml round-bottom flask, weigh out 4-nitrobenzoic acid (0.85 g, 0.005 mol). Add to this 8 ml of absolute ethanol. Add boiling stones, and then bring this solution to the Lab Technologist. WATER OUT b) The Lab Technologist will deliver 1.2 ml of concentrated sulfuric acid to the mixture from the automatic pipette. [CAUTION,...
question 2 and 6 thabk you
Exercises 1. (a) Calculate the volume of 6 M NaOH required to react completely with the amount of methyl salicylate you used. How much of the 6 M NaOH that you used was in excess of the theoretical amount? (b) What volume of 3 M H SO is needed to neutralize all of the disodium salicylate and the excess NaOH present after the initial reaction? How much sulfuric acid was in excess? 2. Refer...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
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