The distance that a spot of a particular compound moves up the
TLC plate relative to the distance moved by the solvent is called
the Rf
value. What does Rf stand for?
a. Refractive factor
b. Reflux fashion
c. Raoult’s factor
d. Retention factor
1 points
QUESTION 2
The components of an immiscible mixture boil at _________________.
a. higher temperatures than the boiling points of the individual components of the mixture
b. a temperature that is exactly in between the boiling point of the individual components of the mixture
c. lower temperatures than the boiling points of the individual components of the mixture
d. the boiling point of water, which is 100°C.
1 points
QUESTION 3
Generally speaking ____________ compounds tend to elute off the column first.
a. polar
b. acidic
c. non-polar
d. basic
QUESTION 4
TLC stands for _____________.
a. Tender Loving Care
b. The Least Concentrated
c. Thin Layer Chromatography
d. The Learning Channel
QUESTION 5
In order for steam distillation to be effective, the organic compounds in the mixture must be _____________.
a. miscible with water
b. less dense than water
c. immiscible with water
d. more dense than water
QUESTION 6
Which one of the following solvents is the most polar?
a. toluene
b. ethanol
c. diethyl ether
d. acetone
QUESTION 7
An efficient separation employing GC include all of the following except_____________.
a. temperature of the column
b. diameter of the column
c. volatility of the compound
d. length of the column
The distance that a spot of a particular compound moves up the TLC plate relative to...
6. Silica gel was used as the solid support for the TLC plate.
Which of the three compounds (A, B, or C) in the APPLIED MIXTURE is
the least polar? (See the figure attached.)
8. Which compound below will have the highest Rf on a TLC
plate? Explain your reasoning. (See figure attached.)
10. The following TLC plates have been spotted with two
different compounds and are about to be eluted. For each plate,
explain if it has been spotted...
Please help
2. Consider the TLC plate shown below that was done on silica gel using a solvent mixture of 4:1 hexane/EtoAc as the eluent. 4:1 Hexane:EtOAC marked solvent front Spot B Spot A A origin (a) Which of the two organic compounds labeled A and B is less polar? (b) Calculate the Rf value of compound B. (c) How would the following changes affect the Rf values of A and B? i. Change to a more polar solvent mixture...
10. On the TLC plate below, identify the spots in the unknown mixture as compound A, B. and C and calculate all Rf values. Lanes with X are unknown sample spots. State whether the solvent system used is a great one for the separation of the compounds. С X В X A
2. An unknown compound was analyzed using thin layer chromatography, its constituted of two components (A and B) as shown in the TLC (Silica coated stationary phase; Chloroform and Ethyl acetate as mobile phase). The mixture was then loaded onto column with silica as the stationary phase and the same solvent system was used. (2 points) Column Chromatography TLC time A В Predict the order of elution of the compounds (A and B). which one would be eluted first/last and...
1. What is the retention factor for the following TLC plate if the baseline is 1 cm, elute solvent traveled 5cm, and the spot of interest traveled 2.5cm? a) 0.50 b) 1.6 c) 0.63 d) 1.4 10. Column chromatography employs both a stationary and a mobile phase. Which of the compounds listed below is commonly used as the stationary phase in column chromatography? a) decolonizing charcoal b) sodium bicarbonate c) benzoic acid d) silica gel
Macros III. Physical Properties 10 pts 10. Place the compounds below in order of increasing melting point. Briefly explain your reasoning VELHO d) e) f) f) 11. Place the same compounds in order of increasing polarity. Briefly explain your reasoning 12. Dichloromethane (methylene chloride CH2C12) is which of the following: i. Water immiscible and more dense than water il Water miscible and more dense than water ili. Water miscible and less dense than water iv. Water immiscible and less dense...
d) Draw the structure of the most polar compound and draw an arrow (through the structure) representing the overall/net dipole moment of the compound. 3) Suppose that your TLC showed that the compounds had not travelled away from your loading spot. What would be an easy condition to change to make the compounds travel up the TLC plate)? Briefly, state specifically what new condition might you try! (0.5) New conditions you could try is dotting more in the same spot,...
Question 11 pts Match the definition with it's correct word. A mixture composed of a solute dissolved in a solvent. [ Choose ] Solute Solution Soluble Miscible Insoluble Solvent Immiscible The greater substance that does the dissolving in a solution. [ Choose ] Solute Solution ...
I need help with questions 1-4. I appreciate all the help.
Thanks!
POST LAB ANALYSIs I. Why do solutions with dissolved salts boil at a higher temperature than the pure solvent? Why do solutions of two miscible liquids boil at a temperature that is in between the boiling point of the components? 2. Why do mixtures of immiscible liquids boil at temperatures lower than the boiling points of the components? 3. 4. For each of the following mixtures, predict the...
Question 9 1 pts Considering the silica gel TLC plate shown, which compound is the most polar (the solvent front is at 4.0 cm)? Spot Distance traveled (cm) A 0.50 В 2.0 IC 3.0 D 1.0 O Compound B (spot B) Compound A (spot A) O Compound D (spot D) O Compound C (spot C)