Question

  

422 (4 pts) Using the flow-chart below, outline a separation of Benzoic acid (s) (1), benzyl amine d) (2), and Naphthalene (s) (3). From the list of procedural steps below, write the letter corresponding to each procedure in the appropriate Ellipse boxes. Each procedure ma once, more than once or not at all. Usi corresponding to each structure in the appropriate square boxes. Each compound may be used once, used ng the compounds drawn below, write the number more than once or not at all. Each square box may contain one or more compounds. Aqueous phasem Aqueous phase Aqueous Phase Mixture of 1, 2,3 D Organic Phase Organic Phase- Organic Phase Compounds (write in the square boxes) 3. Naphthalene ChoHs4. PhCH2NHNa 2. PhCH2NH2 1. PhCOOH 5. PhCOONa 6. PhCH2NH3 Cl 7. PhCOOH2 8. NaCl Procedures (Write in the ellipse boxes) A. Treat with aqueous NaOH B) Treat with dil. HCl C) Vacuum Filteration D. Add Methylene Chloride (Dichloromethane). E) Dilute with water F. Extract with NaCl G. Dry with anhydrous Na2SO4 H. Evaporate Solvent

Please help I need to fill in the blanks by using the compounds and producers below the picture. Thanks!

Answer 1

« thrt« ojven comOovncls denzoie aciol aefs as c weak aci le bnzyl Amine act a at od pkha lene i bial comei dsotdivm bentoc: aeion - base neutralfzafien. on oith HCl becomes profonaledl. owlhq aclol/base - -extmaction fo Separafe îhese compodndi Ueaus Phase IT, with anle C H