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Pre-lab Assignment: Synthesis of Aspirin 1. What is the chemical name for aspirin? 2. How does...
Name Lab Partner LAB 9 REFLECTIVE EXERCISES Lab Section 1 What data did you collect to...
Name Lab Partner LAB 9 REFLECTIVE EXERCISES Lab Section 1 What data did you collect to indicate that you successfully produced aspirin? What did your results indicate about the purity of the aspirin you obtained? Explain your answers. 2 Given that the melting point of salicylic acid is 159 C, can you be certain that the product you isolated was not pure solicylic acid that was unchanged during the reaction? Can you be certain that the product you isolated was...
Experiment 11: Synthesis of Aspirin pre-lab (4 pts) 1) (2 pts) Refer to the introduction on...
Experiment 11: Synthesis of Aspirin pre-lab (4 pts) 1) (2 pts) Refer to the introduction on interpreting the ferric chloride test for phenols. Two students performed the aspirin synthesis experiment. Their melting point and ferric chloride test data are shown below. Based on the results, which student's aspirin has the higher purity? Justify your choice using the melting point data and ferric chloride test results. Melting point range for pure aspirin = 136-140 °C. Melting point range (°C) Ferric chloride...
Preparation of Aspirin Name Class & Section PRE-LABORATORY ASSIGNMENT 1. What hazards should you be aware of wh...
Preparation of Aspirin Name Class & Section PRE-LABORATORY ASSIGNMENT 1. What hazards should you be aware of when working with the following chemicals? a. Acetic anhydride b. Concentrated sulfuric acid 2. Explain the following terms as they relate to this experiment. a. Catalyst b. Limiting reactant 3. Following the procedure described in this experiment, a student reacted 2.775 g of salicylic acid with 4.0 ml of acetic anhydride and recovered 2.986 g of aspirin. a. Calculate the number of moles...
95 Experiment IX Synthesis of Aspirin Prelaboratory Assignment Name: frobect Bun, Bak Baniot Date...
95 Experiment IX Synthesis of Aspirin Prelaboratory Assignment Name: frobect Bun, Bak Baniot Date Sabaitecd Section #. . Using chemical structures, write the balanced equation for the synthesis of aspirin and label all reagents and products with their appropriate names. ooH он C14 14,03 2. What are the two functional groups on salicylic acid? 3. What are the two functional groups on aspirin? b. anhydride? b) How many moles of Apririn could be produced from 2 moles of salicylic acid?...
Fill in the table and answer the questions below Name Pre-lab Questions (10 Marks) 1. Fill...
Fill in the table and answer the questions below
Name Pre-lab Questions (10 Marks) 1. Fill the table below: Materials Acetic anhydride H:SO, Salicylic acid Amount 12mL 0.25 mL 3mL Measured Molecular weight (g/mol) Moles 2. Identify the limiting reagent in this reaction? 3. Calculate the theoretical mass yield of Aspirin product? Show your work for full credit. [4] 4. What is the literature melting point of Aspirin (acetyl salicylic acid)?
please help Mustrates treat all types of ilnesses. Background Aspirin is a prodrug of salicylic acid,...
please help
Mustrates treat all types of ilnesses. Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the andient Greeks as a treatment for pain and fever. Salicylic acid (and many related phenols) are very hard on your Ho stomach, but when esterified, as aspirin is, they are much better tolerated. Simple esters are...
1) Which reactant, salicylic acid or acetic anhydride, is in excess? Show your work. 2) If you we...
1) Which reactant, salicylic acid or acetic anhydride, is in
excess? Show your work.
2) If you were to use 3.17 g of starting material, how much
product would you expect? Again, show your work.
3) Why is phosphoric acid added to the reaction?
4) A small amount of water is added at the end of the reaction
to react with the excess acetic anhydride. Show a balanced equation
for that reaction.
5) Explain the purpose of the FeCl3 test...
DATA Part A: Synthesis of Aspirin Mass of salicylic acid Mass of watch glass Mass of...
DATA Part A: Synthesis of Aspirin Mass of salicylic acid Mass of watch glass Mass of watch glass + dry product Calculated mass of dry product Melting range of product Addition of FeCl, to salicylic acid Addition of FeCl, to product Theoretical yield of aspirin Show calculation: Percent yield of aspina product Show calculation: Lab 9 . Formation o Section LAB 9 REFLECTIVE EXERCISES Date 1 What data did you collect to indicate that you successfully produced aspirn? What did...
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1....
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1. The Synthesis of Aspirin Record the weight of your aspirin, and calculate the percentage yield. Base the yield on salicylic acid since we acetic anhydride was used. Show all calculations. Weight of aspirin d. 08035 Yield of aspirin 2. Contaminants in Aspirin What was the color of the salicylic acid-ferric chloride test solution? On the basis of color is either your aspirin or commercial...
Name Lab Partner Lab Section Date Lab 9 DATA Part A: Synthesis of Aspirin Mass of...
Name Lab Partner Lab Section Date Lab 9 DATA Part A: Synthesis of Aspirin Mass of salicylic acid 1.047 g Mass of watch glass 37.3959 Mass of watch glass + dry product 38.1409 Calculated mass of dry product 0.7459 Melting range of product 136-140 Addition of FeCl, to salicylic acid Addition of FeCl, to product Theoretical yield of aspirin Show calculation: Percent yield of aspirin product Show calculation:
Name Lab Partner LAB 9 REFLECTIVE EXERCISES Lab Section 1 What data did you collect to indicate that you successfully produced aspirin? What did your results indicate about the purity of the aspirin you obtained? Explain your answers. 2 Given that the melting point of salicylic acid is 159 C, can you be certain that the product you isolated was not pure solicylic acid that was unchanged during the reaction? Can you be certain that the product you isolated was...
Experiment 11: Synthesis of Aspirin pre-lab (4 pts) 1) (2 pts) Refer to the introduction on interpreting the ferric chloride test for phenols. Two students performed the aspirin synthesis experiment. Their melting point and ferric chloride test data are shown below. Based on the results, which student's aspirin has the higher purity? Justify your choice using the melting point data and ferric chloride test results. Melting point range for pure aspirin = 136-140 °C. Melting point range (°C) Ferric chloride...
Preparation of Aspirin Name Class & Section PRE-LABORATORY ASSIGNMENT 1. What hazards should you be aware of when working with the following chemicals? a. Acetic anhydride b. Concentrated sulfuric acid 2. Explain the following terms as they relate to this experiment. a. Catalyst b. Limiting reactant 3. Following the procedure described in this experiment, a student reacted 2.775 g of salicylic acid with 4.0 ml of acetic anhydride and recovered 2.986 g of aspirin. a. Calculate the number of moles...
95 Experiment IX Synthesis of Aspirin Prelaboratory Assignment Name: frobect Bun, Bak Baniot Date Sabaitecd Section #. . Using chemical structures, write the balanced equation for the synthesis of aspirin and label all reagents and products with their appropriate names. ooH он C14 14,03 2. What are the two functional groups on salicylic acid? 3. What are the two functional groups on aspirin? b. anhydride? b) How many moles of Apririn could be produced from 2 moles of salicylic acid?...
Fill in the table and answer the questions below
Name Pre-lab Questions (10 Marks) 1. Fill the table below: Materials Acetic anhydride H:SO, Salicylic acid Amount 12mL 0.25 mL 3mL Measured Molecular weight (g/mol) Moles 2. Identify the limiting reagent in this reaction? 3. Calculate the theoretical mass yield of Aspirin product? Show your work for full credit. [4] 4. What is the literature melting point of Aspirin (acetyl salicylic acid)?
please help
Mustrates treat all types of ilnesses. Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the andient Greeks as a treatment for pain and fever. Salicylic acid (and many related phenols) are very hard on your Ho stomach, but when esterified, as aspirin is, they are much better tolerated. Simple esters are...
1) Which reactant, salicylic acid or acetic anhydride, is in
excess? Show your work.
2) If you were to use 3.17 g of starting material, how much
product would you expect? Again, show your work.
3) Why is phosphoric acid added to the reaction?
4) A small amount of water is added at the end of the reaction
to react with the excess acetic anhydride. Show a balanced equation
for that reaction.
5) Explain the purpose of the FeCl3 test...
DATA Part A: Synthesis of Aspirin Mass of salicylic acid Mass of watch glass Mass of watch glass + dry product Calculated mass of dry product Melting range of product Addition of FeCl, to salicylic acid Addition of FeCl, to product Theoretical yield of aspirin Show calculation: Percent yield of aspina product Show calculation: Lab 9 . Formation o Section LAB 9 REFLECTIVE EXERCISES Date 1 What data did you collect to indicate that you successfully produced aspirn? What did...
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1. The Synthesis of Aspirin Record the weight of your aspirin, and calculate the percentage yield. Base the yield on salicylic acid since we acetic anhydride was used. Show all calculations. Weight of aspirin d. 08035 Yield of aspirin 2. Contaminants in Aspirin What was the color of the salicylic acid-ferric chloride test solution? On the basis of color is either your aspirin or commercial...
Name Lab Partner Lab Section Date Lab 9 DATA Part A: Synthesis of Aspirin Mass of salicylic acid 1.047 g Mass of watch glass 37.3959 Mass of watch glass + dry product 38.1409 Calculated mass of dry product 0.7459 Melting range of product 136-140 Addition of FeCl, to salicylic acid Addition of FeCl, to product Theoretical yield of aspirin Show calculation: Percent yield of aspirin product Show calculation:
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