In Exp #2 you added NaOH(aq) to the separatory funnel which contained benzoic acid and naphthalene...
In Exp #2 you added NaOH(aq) to the separatory funnel
which contained benzoic acid and naphthalene in dichloromethane.
Explain the important process that happened at the molecular level
and bulk level in this step. Include solubility considerations in your
answer.
Give your best answer in four sentences or less.
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In Exp #2 you added NaOH(aq) to the separatory funnel
which contained benzoic acid and naphthalene...
Draw the reaction mechanism with chemical structures in the separation of naphthalene and benzoic acid by...
Draw the reaction mechanism with chemical structures in the separation of naphthalene and benzoic acid by extraction. 1g of Naphthalene/benzoic acid mixture is dissolved in 15 mL dichloromethane, transferred to a separatory funnel where 10 mL 2.5M NaOH(aq) is added. Organic and Aqueous layers are separated, and 12M HCl(aq) is added to the aqueous layer while cooling, forming a precipitate, which is vacuum filtrated. Don't understand how to draw each chemical structure!
You have a separatory funnel that contains a solution of 4-methyl benzoic acid and ethoxybenzene in...
You have a separatory funnel that contains a solution of 4-methyl benzoic acid and ethoxybenzene in methylene chloride. By adding KOH (aq) into this solution for extraction, what compound(s) would be expected to form in the aqueous layer? Write the equation. Compound X has a hexane/water distribution coefficient of 2.0. (a) Does compound X have a higher or lower solubility in hexane comparing to water? (b) How much of a 3.0 g sample of compound X dissolved in 100 ml...
1)When you perform a liquid-liquid extraction using a separatory funnel, which of the following organic solvent...
1)When you perform a liquid-liquid extraction using a separatory funnel, which of the following organic solvent is on the bottom of the aqueous phase and which is on top? (write your answer by the solvent name) a) Ethyl acetate b) hexane c) Dichloromethane d) diethyl ether 2) If you are performing a liquid-liquid extraction and you have a mix of a carboxylic acid and a non-acidic compound, which combination of solvents would you use for the separation? a) dichloromethane/HCI b)...
please help :( to the separatory funnel and shake a rate the layers (Step 3), Return...
please help :(
to the separatory funnel and shake a rate the layers (Step 3), Return the mu we aqueous layer with 10 ml of dichloromethane observations in your laboratory notebook dichloromethane layers and return the ane layers and return them to the separatory funne With 10 mL of IM NaOH (Step 8). Describe w OF IM NaOH (Step 8). Describe what happened in yo . Separate the layers (Step 9) and extract the organ e times (Steps 10 -...
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An unknown mixture (dissolved in diethyl ether) contains only 2 of the following : benzoic acid, phenol, aniline and napthalene. You use the acid-base extraction method and want to identify the 2 compounds in your original mixture. 1) To separate the organic acid you add NaOH and to separate the organic base you add HCl.In both cases these extractions are followed by extractions with water. Why do we add water? Why is this step important? (A clear explanation please). 2)When...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction 1. Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below....
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
question 2 and 6 thabk you Exercises 1. (a) Calculate the volume of 6 M NaOH...
question 2 and 6 thabk you
Exercises 1. (a) Calculate the volume of 6 M NaOH required to react completely with the amount of methyl salicylate you used. How much of the 6 M NaOH that you used was in excess of the theoretical amount? (b) What volume of 3 M H SO is needed to neutralize all of the disodium salicylate and the excess NaOH present after the initial reaction? How much sulfuric acid was in excess? 2. Refer...
Construct a flow chart describing the seperation of the mixture and the isolation of each compound...
Construct a flow chart describing the seperation of the
mixture and the isolation of each compound in this experiment. (Lab
steps/procedures includes for reference)
4. Construct a flow chart describing the separation of the mixture and the isolation of each compound in this experiment. A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction...
CHEM 242L Exp. 4 Report/ Synthesis of Oil of Wintergreen Name Score: 20 1) Assess the effectivene...
please answer all these questions, thank you.
CHEM 242L Exp. 4 Report/ Synthesis of Oil of Wintergreen Name Score: 20 1) Assess the effectiveness of the experiment and your technique by A) reporting the yield of each step in grams and percent as well as the overall percent yield (What is "overall percent yield?). SHOW ALL CALCULATIONS! B) Give a complete analysis of the identity and purity of your final product and any isolated intermediates 2 What was the purpose...
You have a separatory funnel that contains a solution of 4-methyl benzoic acid and ethoxybenzene in methylene chloride. By adding KOH (aq) into this solution for extraction, what compound(s) would be expected to form in the aqueous layer? Write the equation. Compound X has a hexane/water distribution coefficient of 2.0. (a) Does compound X have a higher or lower solubility in hexane comparing to water? (b) How much of a 3.0 g sample of compound X dissolved in 100 ml...
1)When you perform a liquid-liquid extraction using a separatory funnel, which of the following organic solvent is on the bottom of the aqueous phase and which is on top? (write your answer by the solvent name) a) Ethyl acetate b) hexane c) Dichloromethane d) diethyl ether 2) If you are performing a liquid-liquid extraction and you have a mix of a carboxylic acid and a non-acidic compound, which combination of solvents would you use for the separation? a) dichloromethane/HCI b)...
please help :(
to the separatory funnel and shake a rate the layers (Step 3), Return the mu we aqueous layer with 10 ml of dichloromethane observations in your laboratory notebook dichloromethane layers and return the ane layers and return them to the separatory funne With 10 mL of IM NaOH (Step 8). Describe w OF IM NaOH (Step 8). Describe what happened in yo . Separate the layers (Step 9) and extract the organ e times (Steps 10 -...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
question 2 and 6 thabk you
Exercises 1. (a) Calculate the volume of 6 M NaOH required to react completely with the amount of methyl salicylate you used. How much of the 6 M NaOH that you used was in excess of the theoretical amount? (b) What volume of 3 M H SO is needed to neutralize all of the disodium salicylate and the excess NaOH present after the initial reaction? How much sulfuric acid was in excess? 2. Refer...
Construct a flow chart describing the seperation of the
mixture and the isolation of each compound in this experiment. (Lab
steps/procedures includes for reference)
4. Construct a flow chart describing the separation of the mixture and the isolation of each compound in this experiment. A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction...
please answer all these questions, thank you.
CHEM 242L Exp. 4 Report/ Synthesis of Oil of Wintergreen Name Score: 20 1) Assess the effectiveness of the experiment and your technique by A) reporting the yield of each step in grams and percent as well as the overall percent yield (What is "overall percent yield?). SHOW ALL CALCULATIONS! B) Give a complete analysis of the identity and purity of your final product and any isolated intermediates 2 What was the purpose...
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