[(+)-Co(en)3]I3•H2O Preparation
Could you help me understand why this reaction happens for this procedure: dissolve [(+)-Co(en)3][(+)-tart]Cl•5H2O in 15 mL of warm water and add 0.25 mL of concentrated ammonia (15 M) solution. With stirring, add a solution of 17.0 g of NaI in 7 mL hot water. After cooling in an ice-water bath, filter the product using vacuum filtration and wash the crystals with an ice cold solution of 3.00 g of NaI in 10 mL of water. Wash the produce with ethanol and then acetone, air dry [(+)-Co(en)3]I3•H2O.
So how does adding NH3 and NaI convert [(+)-Co(en)3][(+)-tart]Cl•5H2O to [(+)-Co(en)3]I3•H2O. ? pls explain in detail....thank you!
[(+)-Co(en)3]I3•H2O Preparation Could you help me understand why this reaction happens for this procedure: dissolve [(+)-Co(en)3][(+)-tart]Cl•5H2O...
Please help! (These are the instructions I had) 1) Preparation of K2[Cu(C2O4)2] 2H2O CuSO4•5H2O + 2K2C2O4•H2O → K2[Cu(C2O4)2]•2H2O + K2SO4 + 5H2O Heat a solution of 2.5g of potassium oxalate monohydrate in 12.5mL of water contained in a 50mL beaker (approx. 90°C). Heat 1.55g of copper sulfate pentahydrate in 3mL of water to about 90°C and add it rapidly, with vigorous stirring to the hot potassium oxalate solution. Set on the bench and allow to cool to room temperature then...
I understand that equivalents is the ratio of the # of moles
of a reactant or reagent compared to the # of moles of the
substrate. But I am confused on how to answer this question and why
the procedure would call for more NaI than Vanillin if Vanillin is
the substance needed substituted. Can you help?
Thanks!
3. How many equivalents of sodium iodide are used in this experiment? Show your calculation Speculate about why the procedure calls for...
Determine the theoretical yield and limiting reagent
Running the Reaction Add 0.100 g benzil and 0.30 mL 95% ethanol to a 3-mL conical vial. Place a spin vane in the vial and attach an air condenser. Heat the mixture with an aluminum block (90-100°C) while stirring until the benzil has dissolved (see inset in Tech- nique 6, Figure 6.1A). Using a 9-inch Pasteur pipette, add dropwise 0.25 mL of an aqueous potassium hydroxide solution' downward through the condenser into the...
You
don’t have to tell me purpose. just where in procedure for each
technique.
Section/Instructor SN2 Pre-lab (20 points) Answer on a separate piece of paper 1. (6 pts.) What is the purpose of the following experimental techniques and where in the procedure is each used? a. Heating under reflux b. Simple distillation c. Water wash d. Addition of COLD NAOH e. Saturated NaCl solution f. Addition of anhydrous sodium sulfate SN2 Reaction Procedure Set-Up: 100 mL RBF: 11.1 g...
How can the NMP oxalate salt be converted back to NMP? Here is the procedure: PROCEDURES Part A: Synthesis of (±)-N,N-dimethyl-3-phenyl-3-(4-trifluoromethylphenoxy)propanamine To the 250-mL round-bottom flask (RBF) containing (±)-3-(dimethylamino)-1-phenylpropanol (product from Lab 6) and a magnetic stir bar, add 4 mL of 4-chlorobenzotrifluoride and 30 mL of dimethylacetamide (DMA). With stirring, add to this mixture 30 mL of 1.0 M potassium tert-butoxide (caustic alkali!) in tert-butyl alcohol using a syringe. Using a simple distillation apparatus, distill the mixture slowly, with...
I need help calculating theoretical yield for my
Diels-Alder lab experiment. This reaction was between 1,3-butadiene
and maleic anhydride, forming cis 1,2,3,6-tetrahydrophthalic
anhydride. In this experiment 1.0g of maleic anhydride was combined
with 1.8g 3-sulfolene and 2 mL dry xylene and refluxed for 30 mins.
6 mL of xylene was added to dissolve solids and then decanted, then
warm pet. ether was added to form crystalline product after
cooling. some of this info may be irrelevant in what is needed...
The first picture is used for question #2, and question #3 can
be normally answered. I believe the answer to question 3 is ->
0.07144M. However I would like someone to check it. I am not sure
about 2.
BE SURE THAT YOU RECORD ALL OF YOUR DATA AND LABEL PROPERLY FOR PARTI OF THIS LABORATORY EXPERIMENT. YOU WILL NEED TO ACCESS THIS INFORMATION IN THREE WEEKS. Part I Synthesis of the Complex Salt containing Copper Procedure 16.004 1. In...
Pre-Lab Assignment
1) Draw the reaction mechanism for the reaction.
2) Determine the limiting reagent.
Procedure 1 Place approximately 1 g of stilbene dibromide prepared in last week's experiment in a 50 mL round bottom flask. Record the exact mass. Add 0.8 g of KOH and 4 mL of triethylene glycol from the syringe provided in the fume hood (rinse any crystals from the sides of the flask while adding triethylene glycol). 2 Heat the stirred reaction mixture to a...
1. In order for a solution to generate heat when irradiated by
microwaves the solvent must have?
2. Identify what the solvent is for this reaction. Draw its
structure.
cetyl anthranilic acid into a large, dry, test tube place 0.68 g of anthranilic acid, 2.2 mL of acetic anhydride and a Doung chip. Upon the addition of the acetic anhydride the tube may become warm. Swirl the tubo brany to mix the reagents. Place the tube into a beaker. Place...
i need help answering the questions plz and thanks!
Experiment 9 Report Sheet: Calculations and Questions Calculations 1. Determine which of the two starting materials is the limiting reagent, then determine the theoretical yield of [Cu(NH3)]SO4+H20. 2. Determine the percent yield after the first crystallization. Is this a valid percent yield? Explain. 3. Determine the percent yield of the second crystallization. Conclusion On the back of this page write a conclusion that comments on what you were trying to accomplish...