Please help me with this question. Thank you so much!
A 0.5-mL sample of the filtered crude pig heart extract was removed and was labeled “CRUDE.” 30.0 mL of filtered crude pig heart extract was added to a clean beaker and gently stirred on ice using a magnetic stir bar. This solution was kept ice cold throughout. Finely crushed ammonium sulfate powder was slowly added to the crude extract until the solution was 40% saturated.
1). Assuming a solubility of 70.6 g of ammonium sulfate per 100 mL of H2O at 0.00°C (ice-cold solution), how many grams of ammonium sulfate must be added to the crude extract to bring the solution to 40% saturation?
Please help me with this question. Thank you so much! A 0.5-mL sample of the filtered...
As it says in question 2 could you please help me make a flow
chart like the provided example below?
2) For the portion of the procedure shown below, create a flow chart for the acid-base extraction at the end of the Grignard Reaction in a similar manner to the one on Canvas for the extraction lab. Start your flow chart with the crude reaction mixture before addition of HCl and continue it until the product is recovered. Depict the...
You
don’t have to tell me purpose. just where in procedure for each
technique.
Section/Instructor SN2 Pre-lab (20 points) Answer on a separate piece of paper 1. (6 pts.) What is the purpose of the following experimental techniques and where in the procedure is each used? a. Heating under reflux b. Simple distillation c. Water wash d. Addition of COLD NAOH e. Saturated NaCl solution f. Addition of anhydrous sodium sulfate SN2 Reaction Procedure Set-Up: 100 mL RBF: 11.1 g...
If each bag of Lipton black tea contains 55 mg of caffeine, what is the maximum amount of caffeine that you could extract from one using our procedure? Assume one bag and 40mL of tea-water at the end of initial solid-liquid extraction. The partition coefficient (K) for caffeine in methylene chloride is 7.2. How much caffeine could be extracted using our procedure if we had used ethyl acetate (K = 2.0) instead of methylene chloride? Explain why the amount does...
please help me with 3,4,5
Thank you!
3. Which sample had more moles of HA in it initially? Give reas on ! 4. Do the prelab calculation found in part IIIA below 5. Calculate the (expected) initial concentration of your acid solution (see Part IIIB below to get the initial volume of your acid solution) Acid 2 0 50 40 30 0 10 20 Volume of titrant (base) added (mL) III. Experimental Information and Procedures A.Background and preliminary calculation. You...
i need help answering the questions plz and thanks!
Experiment 9 Report Sheet: Calculations and Questions Calculations 1. Determine which of the two starting materials is the limiting reagent, then determine the theoretical yield of [Cu(NH3)]SO4+H20. 2. Determine the percent yield after the first crystallization. Is this a valid percent yield? Explain. 3. Determine the percent yield of the second crystallization. Conclusion On the back of this page write a conclusion that comments on what you were trying to accomplish...
Please help! (These are the instructions I had) 1) Preparation of K2[Cu(C2O4)2] 2H2O CuSO4•5H2O + 2K2C2O4•H2O → K2[Cu(C2O4)2]•2H2O + K2SO4 + 5H2O Heat a solution of 2.5g of potassium oxalate monohydrate in 12.5mL of water contained in a 50mL beaker (approx. 90°C). Heat 1.55g of copper sulfate pentahydrate in 3mL of water to about 90°C and add it rapidly, with vigorous stirring to the hot potassium oxalate solution. Set on the bench and allow to cool to room temperature then...
i need help with #3 please!
SAFETY NOTES: Bromobenene and acetophenone are irritants. Wear gloves and avoid contact with skin, eyes, and clothing • MHC) is dritating to the skin avoid contact with the skin, eyes, and clothing Diethyl ether, usually referred to simply as "ether", is volatile and flammable. Keep a safe distance from hot electrical devices WASTE DISPOSAL *** A itrate is the liquid that passed through the Hirsch funnel, ending up in the bottom of the sidearm...
Organic chemistry post-lab question: "Why is important
to add the alkyl halide dropwise in your reaction? (Hint: your
reaction is not heated, but you still need a water-cooled
condenser!)" Please answer in detail!
Here is a copy of the experiment, thank you!
The Grignard reaction is an important synthetic process by which a carbon-carbon bond is formed. Magnesium metal is first reacted with an organic halide. The resultant organo-magnesium halide (Grignard reagent) is then combined with a carbonyl compound, ultimately...
hi, please help me with number 7. thank you
EXPERIMENT SEVEN SODIUM BOROHYDRIDE REDUCTION OF ACETOPHENONE HOCH, DISCUSSION The reduction of an aldehyde or ketone with sodium borohydride is straight forward and usually affords a high yield of the alcohol. The usual procedure (and the one employed in this experiment) involves dissolving the borohydride in 95% ethanol and adding the carbonyl compound to this solution. To ensure complete reaction, an excess of sodium borohydride is used. The reaction between sodium...
please help me answer those three questions according to the
oother pictures
į CH, CH3 1. NaOMe in MeOH / EtOH, reflux 2. Ethyl lodide, reflux N bolo OH Acetaminophen phenacetini erot!) DAN Procedure: Measure and dispense 0.6 ml of a 4.4 M solution of sodium methoxide in methanol and im of ethanol into a 5 mL reaction vial. Add 215 mmol of acetaminophen (-0.378 8). Set up for reflux in the Tume hood and bring reaction to reflux for...